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Beilstein J. Org. Chem. 2016, 12, 1453–1458, doi:10.3762/bjoc.12.141
Graphical Abstract
Figure 1: Synthetic overview of “NU-BIPHEP(O)s”. A) Rhodium catalyzed double [2 + 2 + 2] cycloaddition. B) Ac...
Figure 2: Investigation of 3,5-dichlorobenzoyl modified tetrahydrobiisoindole “NU-BIPHEP(O)” 3. A) Three sign...
Figure 3: Investigation of “NU-BIPHEP(O)” 1b. A) Solid-state structure determined by X-ray crystallography. H...
Figure 4: Enantioselective DHPLC investigation of tetrahydrobiisoindole “NU-BIPHEP(O)” 3. A) Elution profiles...
Beilstein J. Org. Chem. 2014, 10, 701–706, doi:10.3762/bjoc.10.63
Scheme 1: Synthesis of formamide 4. Reagents and conditions: a) KHMDS, THF, −78 °C; then: NaBH4, MeOH, 63%. b...
Figure 1: Equilibration of the Z-rotamer of 4 at 293 K.
Figure 2: Equilibration of the E-rotamer of 4 at 293 K.
Figure 3: Elution profiles obtained by temperature-dependent DHPLC measurements of 4.
Figure 4: Eyring plot obtained by temperature dependent DHPLC measurements of 4.
Figure 5: Potential energy surface scan graph for the dihedral angle O–C–N–C1 () in 4 (BP-D3/def2-SVP).
Figure 6: Energy differences and geometries for E- and Z-4 and both transition states (TS1 and TS2) in hexane...
Beilstein J. Org. Chem. 2013, 9, 1837–1842, doi:10.3762/bjoc.9.214
Figure 1: Overview of some capabilities of an immobilized or in an inert stationary phase dissolved catalyst....
Scheme 1: Diels–Alder reaction of benzenediazonium-2-carboxylate with anthracene-9-derivatives toward triptyc...
Figure 2: The experimental setup and a) the injection sequence protocol of the cryogenic ocRGC measurements b...
Figure 3: Experimental ocRGC chromatogram of 9-anthracenemethanol with benzenediazonium-2-carboxylate. Condit...